The University of Southern Mississippi

Department of Chemistry and Biochemistry

CHE 311 Analytical Chemistry

 

 

Image result for Fundamentals of Analytical Chemistry

TEXTBOOK : DA. Skoog, DM. West, FJ Holler, and SR. Crouch, Fundamentals of Analytical Chemistry, 9th Ed., Brooks/Cole, 2014.

Videos of Lecture Notes

0. Introductory Video

 

1. Introduction of Analytical Chemistry


Part I: TOOLS OF ANALYTICAL CHEMISTRY.
2. Chemicals, Apparatus, and Unit Operations of Analytical Chemistry.
3. Using Spreadsheets in Analytical Chemistry.
4. Calculations Used in Analytical Chemistry.
5. Errors in Chemical Analyses.
6. Random Errors in Chemical Analysis.
7. Statistical Data Treatment and Evaluation.
8. Sampling, Standardization and Calibration: Part I

8. Sampling, Standardization and Calibration: Part II
 

Part II: CHEMICAL EQUILIBRIA.
9. Aqueous Solutions and Chemical Equilibria: Part I

9. Aqueous Solutions and Chemical Equilibria: Part II

9. Aqueous Solutions and Chemical Equilibria: Part III
10. Effect of Electrolytes on Chemical Equilibria.

10. Solutions of Selected Questions in Chapter 10 Quiz
11. Solving Equilibrium Problems for Complex Systems.

 
Part III: CLASSICAL METHODS OF ANALYSIS.
12. Gravimetric Methods of Analysis.
13. Titrimetric Methods; Precipitation Titrimetry.
14. Principles of Neutralization Titrations.

14A. Review of Chapter 14.

14B. How to Use Excel to Calculate and Plot Acid-Base Titration Curves
15. Titration Curves for Complex Acid/Bases Systems: Part I

15. Titration Curves for Complex Acid/Bases Systems: Part II

15. Titration Curves for Complex Acid/Bases Systems: Part III

15 IV—Using Excel to Calculate Alpha Values of H3PO4
16. Applications of Neutralization Titrations.
17. Complexation Reactions and Titrations.
 

Part IV: ELECTROCHEMICAL METHODS.
18. Introduction to Electrochemistry.
19. Applications of Standard Electrode Potentials.
20. Applications of Oxidation/Reduction Titrations.
21. Potentiometry.
22. Bulk Electrolysis: Electrogravimetry and Coulometry.
23. Voltammetry.


Part V: SPECTROCHEMICAL ANALYSIS.
24-28. Spectrochemical Methods.


Part VI: KINETICS AND SEPARATIONS.
29. Mass Spectrometry.

30. Kinetic Methods of Analysis.
31. Introduction to Analytical Separations.
32. Gas Chromatography.
33. High-Performance Liquid Chromatography.
34. Miscellaneous Separation Methods.
 

Part VII: PRACTICAL ASPECTS OF CHEMICAL ANALYSIS.
35. Analysis of Real Samples.
36. Preparing Samples for Analysis.
37. Decomposing and Dissolving the Sample.
38. Selected Methods of Analysis.

CHE 311 Exams Solution

1. CHE 311 Exam 1 (Chapters 1-8)

2. CHE 311 Exam 2 (Chapters 9-12)

3. CHE 311 Exam 3 (Chapters 13-17)

 

ACS Review

1.   ACS Review Q9 Solution

2.   ACS Review Q35 Solution

3.   ACS Review Q40 Solution

4.   ACS Review Q46 Solution

5.   ACS Review Q51 Solution